Analysis Temperature Guidelines

The guidelines are applicable to all analysis types.

  • Starting Temperature. Experiments should be started at a temperature that is lower than that at which the reaction begins. If the reaction begins below ambient temperature, use the optional CryoCooler.
  • Maximum Temperature. The experiment’s maximum temperature is limited to the temperature at which the sample sinters.
  • Ramp Rate. The recommended ramp rate is 5-10 °C/min, however a different ramp rate can be specified. For example, if using 500 °C as the starting temperature of the reaction, it is more expedient to ramp the temperature rapidly (for example, 50 °C/min.) to a value near 500 °C, then proceed with the experiment at 5-10 ºC/min.
 
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